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Evidence for superplasticity in a CoCrFeNiMn high-entropy alloy processed by high-pressure torsion

机译:高压扭转加工CoCrFeNimn高熵合金的超塑性证据

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摘要

A CoCrFeNiMn high-entropy alloy was processed by high-pressure torsion to produce a grain size of ~10 nm and then tested in tension at elevated temperatures from 773 to 1073 K using strain rates in the range from 1.0×10?3 to 1.0×10?1 s?1. The alloy exhibited excellent ductility at these elevated temperatures including superplastic elongations with a maximum elongation of >600% at a testing temperature of 973 K. It is concluded that the formation of precipitates and the sluggish diffusion in the HEA inhibit grain growth and contribute to a reasonable stability of the fine-grained structure at elevated temperatures. The results show the activation energy for flow matches the anticipated value for grain boundary diffusion in nickel but the strain rate sensitivity is low due to the occurrence of some grain growth at these high testing temperatures
机译:通过高压扭转处理CoCrFeNiMn高熵合金以产生〜10 nm的晶粒尺寸,然后在773至1073 K的高温下使用1.0×10?3至1.0×的应变速率进行张力测试10?1 s?1。该合金在这些高温下表现出出色的延展性,包括超塑性伸长率,在973 K的测试温度下最大伸长率> 600%。结论是,析出物的形成和HEA中缓慢的扩散抑制了晶粒的生长并有助于晶粒的长大。细粒结构在高温下具有合理的稳定性。结果表明,流动的活化能与镍中晶界扩散的预期值匹配,但由于在这些较高的测试温度下出现了一些晶粒长大,因此应变速率敏感性较低

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